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热销推荐:N,N-二甲胺基溴乙烷氢溴酸盐(2862-39-7)

别名:N,N-二甲胺基溴乙烷氢溴酸盐
英文名称:2-(Dimethylamino)Ethyl Bromide Hydrobromide
分子式:C4H11Br2N
Cas No.:2862-39-7
分子量:232.94
结构式:image.png

规格:95%

外观:白色固体

用途:基础原料、有机中间体、医药中间体

合成工艺如下:

potassium carbonate; N,N-dimethyl-formamide;

Reactants are commercially availlable.
General procedure: Corresponding hetrocyclic compounds (0.01 mol), 1,2-dibromoethane (0.01 mol) and anhydrous potassium carbonate (1 g, 0.01 mol) in dry dimethyl formamide (50 mL) were heated under re flux for 6-8 hours, then cooled to room temperature and poured into crushed ice (? 100 g). The precipitated product was filtered off, washed with water, dried and recrystallized from ethanol. Differen t hetrocyclic compounds namely methylpiperazine, ethylpiperazine, triazole, imidazole, indole, benzimidazole and 2-amino pyridine were yielded.


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